Implementation of liquid chromatography tandem mass spectrometry for the analysis of ciguatera fish poisoning in contaminated fish samples from Atlantic coasts Food Chemistry 280 (2019) 8–14 - Download document
LC-MS/MS method for determination of Caribbean Ciguatoxins - Download document
Report Interlaboratory validation Lipophilic toxins by LCMSMS EURLMB - Download document
METHOD FOR QUANTITATIVE DETERMINATION OF MARINE LIPOPHILIC TOXINS IN SHELLFISH USING LC-MS/MS
August 2011
Standard Operating Procedures method for the quantitative determination of marine lipophilic toxins in shellfish using LC-MS/MS.
H.J. van den Top, A. Gerssen, P. McCarron, H.P. van Egmond. Quantitative determination of marine lipophilic toxins in mussels, oysters and cockles using liquid chromatography-mass spectrometry: inter-laboratory validation study. Food Additives & Contaminants: Part A , 2011, Vol. 28, Iss. 12.
METHOD FOR DETECTION OF OKADAIC ACIDTOXINS GROUP IN EDIBLE MOLLUSCS Rev 4
October 2010
Standard Operating Procedures method for the quantitative determination of OA and other carboxylic toxins of the OA group including DTX1, DTX2, DTX3 by a colorimetric phosphatase inhibition assay.
The OkaTest method fulfils the requirements of Chapter III A (4) a, b, and c of Annex III to Regulation (EC) 2074/2005 and can be used as supplementary method to EU-RL LC/MS/MS method only for the detection of Okadaic Acid group toxins OA, DTX1,DTX2, DTX3 including their esters.
The use of OkaTest method is not an alternative to the EU-RL LC/MS/MS method.
Download document (PDF, 101 Kb)
Download document (PDF, 352 Kb)
EN 14176.2017
Determination of Domoic acid in raw shellfish, raw finfish and cooked mussels by RP-HPLC using UV detection
EN 16204. 2012
Determination of lipophilic algal toxins (okadaic acid, yessotoxins, azaspiracids, pectenotoxins) in shellfish and shellfish products by LC-MS/MS
EN 14526.2017
Determination of saxitoxin-group toxins in shellfish
HPLC method using pre-column derivatization with peroxide or periodate oxidation